Comparison between conventional and microwave-assisted hydrodistillation at different power levels has been applied for the extraction of essential oil from Zingiber officinale Rosc. rhizome. In addition to the collected essential oils, as the main products, hydrolats were also collected, as valuable by-products from both extraction techniques. A comparison of two applied techniques was done in terms of extraction time, extraction yield, the chemical composition of essential oils and hydrolats, and environmental impact. Microwave-assisted hydrodistillation achieved a higher extraction yield (1.70, 1.70, and 1.85 % for power levels of 180, 360, and 600 W, respectively) compared to hydrodistillation (1.50 %). Furthermore, distillation time related to the energy consumption has been reduced from 144 min and 1.44 kWh for conventional hydrodistillation to 37, 32, 27 min and 0.11, 0.19, 0.27 kWh for power levels of 180, 360, and 600 W, respectively. Content of α-zingiberene in essential oil and hydrolat obtained by hydrodistillation was 29.89 and 6.87 %, while content of α-zingiberene in essential oils and hydrolats obtained by microwave-assisted hydrodistillation was higher yielding the amounts of 34.12, 34.43, and 42.00 % and 18.70, 22.60, and 32.92 % for power levels of 180, 360, and 600 W, respectively. Microwave-assisted hydrodistillation has proven to be promising technique for the isolation of ginger’s essential oil regarding improved yield, reduced time and energy requirements, as well CO2 emissions while maintains oil quality.
Adams, R. P. (2007). Identification of essential oil components by Gas Chromatography/Mass Spectroscopy. Allured Publishing Corporation.
Drinić, Z., Pljevljakušić, D., Živković, J., Bigović, D., & Šavikin, K. (2020). Microwave-assisted extraction of O. vulgare L. spp. hirtum essential oil: Comparison with conventional hydro-distillation (Vol. 120, pp. 158–165). https://doi.org/10.1016/j.fbp.2020.01.011
Ferhat, M. A., Meklati, B. Y., Smadja, J., & Chemat, F. (2006). An improved microwave Clevenger apparatus for distillation of essential oils from orange peel (Vol. 1112, Issues 1–2, pp. 121–126). https://doi.org/10.1016/j.chroma.2005.12.030
Ferhat, M. A., Tigrine-Kordjani, N., Chemat, S., Meklati, B. Y., & Chemat, F. (2007). Rapid Extraction of Volatile Compounds Using a New Simultaneous Microwave Distillation: Solvent Extraction Device (Vol. 65, Issues 3–4, pp. 217–222). https://doi.org/10.1365/s10337-006-0130-5
Filly, A., Fernandez, X., Minuti, M., Visinoni, F., Cravotto, G., & Chemat, F. (2014). Solvent-free microwave extraction of essential oil from aromatic herbs: From laboratory to pilot and industrial scale (Vol. 150, pp. 193–198). https://doi.org/10.1016/j.foodchem.2013.10.139
Golmakani, M.-T., & Rezaei, K. (2008). Comparison of microwave-assisted hydrodistillation withthe traditional hydrodistillation method in the extractionof essential oils from Thymus vulgaris L. (Vol. 109, Issue 4, pp. 925–930). https://doi.org/10.1016/j.foodchem.2007.12.084
Govindarajan, V. S., & Connell, D. W. (1983). Ginger — chemistry, technology, and quality evaluation: Part 1 (Vol. 17, Issue 1, pp. 1–96). https://doi.org/10.1080/10408398209527343
Hochmuth, D. (2006). Massfinder 3: Softwarefor GC/MS Interpretation and Presentation. Mass Spectral Library Administration, Hamburg, Germany.
Kamaliroosta, Z., Kamaliroosta, L., & Elhamirad, A. (2013). Isolation and identification of ginger essential oil. Journal of Food Biosciences and Technology, 3, 73–80.
Karakaya, S., El, S. N., Karagozlu, N., Sahin, S., Sumnu, G., & Bayramoglu, B. (2014). Microwave-assisted hydrodistillation of essential oil from rosemary (Vol. 51, Issue 6, pp. 1056–1065). https://doi.org/10.1007/s13197-011-0610-y
Paolini, J., Leandri, C., Desjobert, J.-M., Barboni, T., & Costa, J. (2008). Comparison of liquid–liquid extraction with headspace methods for the characterization of volatile fractions of commercial hydrolats from typically Mediterranean species (Vol. 1193, Issues 1–2, pp. 37–49). https://doi.org/10.1016/j.chroma.2008.04.021
PhEur10.0. (2019). European Pharmacopoeia, 10(0.).
Radivojac, A., Bera, O., Micić, D., Đurović, S., Zeković, Z., Blagojević, S., & Pavlić, B. (2020). Conventional versus microwave-assisted hydrodistillation of sage herbal dust: Kinetics modeling and physico-chemical properties of essential oil (Vol. 123, pp. 90–101). https://doi.org/10.1016/j.fbp.2020.06.015
Ravi Kiran, C., Chakka, A. K., Padmakumari Amma, K. P., Nirmala Menon, A., Sree Kumar, M. M., & Venugopalan, V. V. (2013). Essential oil composition of fresh ginger cultivars from North-East India (Vol. 25, Issue 5, pp. 380–387). https://doi.org/10.1080/10412905.2013.796496
REZVANPANAH, S., REZAEI, K., RAZAVI, S. H., & MOINI, S. (2008). Use of Microwave-assisted Hydrodistillation to Extract the Essential Oils from Satureja hortensis and Satureja montana (Vol. 14, Issue 3, pp. 311–314). https://doi.org/10.3136/fstr.14.311
Rezvanpanah, S., Rezaei, K., Razavi, S. H., & Moini, S. (2008). Use of Microwave-assisted hydrodistillation to extract the essentialoils from.
Shahani, S., Monsef-Esfahani, H. R., Hajiaghaee, R., & Gohari, A. R. (2011). Chemical Composition of Essential Oil and Hydrolat ofGeum iranicumKhatamaz (Vol. 23, Issue 6, pp. 29–33). https://doi.org/10.1080/10412905.2011.9712278
Stoyanova, A., Konakchiev, A., Damyanova, S., Stoilova, I., & Suu, P. T. (2006). Composition and Antimicrobial Activity of Ginger Essential Oil from Vietnam (Vol. 9, Issue 1, pp. 93–98). https://doi.org/10.1080/0972060x.2006.10643478
Talebi, M., İlgün, S., Ebrahimi, V., Talebi, M., Farkhondeh, T., Ebrahimi, H., & Samarghandian, S. (2021). Zingiber officinale ameliorates Alzheimer’s disease and Cognitive Impairments: Lessons from preclinical studies (Vol. 133, p. 111088). https://doi.org/10.1016/j.biopha.2020.111088
Tóth, B., Lantos, T., Hegyi, P., Viola, R., Vasas, A., Benkő, R., Gyöngyi, Z., Vincze, Á., Csécsei, P., Mikó, A., Hegyi, D., Szentesi, A., Matuz, M., & Csupor, D. (2018). Ginger (Zingiber officinale): An alternative for the prevention of postoperative nausea and vomiting. A meta-analysis (Vol. 50, pp. 8–18). https://doi.org/10.1016/j.phymed.2018.09.007
Veggi, P. C., Martinez, J., & Meireles, M. A. A. (2012). Fundamentals of Microwave Extraction (pp. 15–52). https://doi.org/10.1007/978-1-4614-4830-3_2
Vinatoru, M., Mason, T. J., & Calinescu, I. (2017). Ultrasonically assisted extraction (UAE) and microwave assisted extraction (MAE) of functional compounds from plant materials (Vol. 97, pp. 159–178). https://doi.org/10.1016/j.trac.2017.09.002
(1984). Pharmacopoea Jugoslavica.
Citation
Copyright
This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
The statements, opinions and data contained in the journal are solely those of the individual authors and contributors and not of the publisher and the editor(s). We stay neutral with regard to jurisdictional claims in published maps and institutional affiliations.